Details
Butyl hydroxyacetate Good Manufacturer supply High Quality 7397-62-8
- Molecular Formula: C6H12O3
- Molecular Weight: 132.159
- Appearance/Colour: clear liquid
- Vapor Pressure: 0.227mmHg at 25°C
- Melting Point: -26ºC
- Refractive Index: 1.427
- Boiling Point: 183 °C at 760 mmHg
- PKA: 12.99±0.10(Predicted)
- Flash Point: 71.7 °C
- PSA： 46.53000
- Density: 1.027 g/cm3
- LogP: 0.32200
Butyl hydroxyacetate(Cas 7397-62-8) Usage
|
Purification Methods |
Dissolve in CHCl3 (EtOH-free), wash with 5% KHCO3 until effervescence ceases (if free acid is present), dry over CaCl2, filter, evaporate and distil through a short column. [B.hme & Opfer Z Anal Chem 139 255 1953, Filachione et al. J Am Chem Soc 73 5265 1951, Beilstein 3 IV 589.] |
|
General Description |
Butyl glycolate is a glycolic acid derivative. |
InChI:InChI=1/C6H12O3/c1-2-3-4-9-6(8)5-7/h7H,2-5H2,1H3
7397-62-8 Relevant articles
Preparation method of glycolic acid or glycolate
-
Paragraph 0148-0150, (2020/09/20)
The invention discloses a preparation me...
Retention Characteristics and Sorption Enthalpies of Esters of Natural Hydroxycarboxylic Acids on DB-1 Stationary Phase
Portnova,Yamshchikova, Yu. F.,Krasnykh
, p. 577 - 583 (2019/06/03)
Abstract: Sorption characteristics and r...
Preparation method of chlorophenoxyacetic ester
-
Paragraph 0046; 0047, (2019/01/08)
The invention provides a preparation met...
Hydroxy acetic acid n-butyl catalytic synthesis method
-
Paragraph 0031; 0032; 0033; 0034; 0035; 0036; 0037-0049, (2017/09/23)
The invention belongs to the technical f...
7397-62-8 Process route
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-
79-14-1
glycolic Acid
-
-
71-36-3
butan-1-ol
-
-
502-97-6
glycolide
-
-
7397-62-8
butyl glycolate
| Conditions | Yield |
|---|---|
|
With
toluene-4-sulfonic acid;
In
cyclohexane;
for 5h;
Reflux;
|
85.1%
|
-
-
50-00-0,30525-89-4,61233-19-0
formaldehyd
-
-
201230-82-2
carbon monoxide
-
-
71-36-3
butan-1-ol
-
-
7397-62-8
butyl glycolate
| Conditions | Yield |
|---|---|
|
formaldehyd; carbon monoxide;
With
1,3,5-Trioxan; formic acid; sulfuric acid;
In
1,4-dioxane; dichloromethane;
at 120 ℃;
under 67506.8 Torr;
butan-1-ol;
In
1,4-dioxane; dichloromethane;
at 160 ℃;
for 40h;
under 18001.8 Torr;
|
98.3%
|
7397-62-8 Upstream products
-
50-00-0
formaldehyd
-
71-36-3
butan-1-ol
-
79-14-1
glycolic Acid
-
502-97-6
glycolide
7397-62-8 Downstream products
-
93759-10-5
[(2,4,5-trichloro-phenoxy)-acetoxy]-acetic acid butyl ester
-
109-11-5
morpholine-3-one
-
54145-95-8
3-methyl-4-oxo-trans -crotonic acid butyl ester
-
5236-64-6
(2,4-Dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-acetic acid butyl ester