Details
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1.What is the CHLOROMETHYL PHENYL SULFIDE ?
Reagent for the high-yield thiomethylation of O-silylated lactone and ester enolates in the synthesis of α-methylene lactones and esters.
-
-
50-00-0,30525-89-4,61233-19-0
formaldehyd
-
-
108-98-5
thiophenol
-
-
7205-91-6
phenylthiomethyl chloride
| Conditions | Yield |
|---|---|
|
formaldehyd;
With
hydrogenchloride;
In
water; toluene;
at 40 ℃;
for 1h;
thiophenol;
In
water; toluene;
at 60 ℃;
for 2h;
|
81%
|
|
With
hydrogenchloride;
In
icosane; toluene;
at 20 - 50 ℃;
for 5h;
|
73%
|
|
With
hydrogenchloride;
at 40 - 60 ℃;
for 2.5h;
|
71%
|
|
With
hydrogenchloride;
at 40 ℃;
for 1.5h;
|
15.1%
|
|
Einleiten von HCl;
|
|
|
With
hydrogenchloride;
In
dichloromethane;
Yield given;
|
|
|
With
hydrogenchloride;
In
toluene;
at 50 ℃;
|
|
|
With
hydrogenchloride;
In
water; toluene;
at 20 - 50 ℃;
for 3h;
|
|
|
formaldehyd;
With
hydrogenchloride;
In
water; toluene;
at 50 ℃;
for 0.166667h;
Inert atmosphere;
thiophenol;
In
water; toluene;
at 20 - 50 ℃;
for 4.75h;
Inert atmosphere;
|
-
-
100-68-5
methyl-phenyl-thioether
-
-
7205-91-6
phenylthiomethyl chloride
| Conditions | Yield |
|---|---|
|
With
N-chloro-succinimide;
In
tetrachloromethane;
for 11h;
Ambient temperature;
|
99%
|
|
With
N-chloro-succinimide;
In
tetrachloromethane;
at 20 ℃;
for 11h;
|
98%
|
|
With
sulfuryl dichloride;
In
dichloromethane;
for 3h;
Inert atmosphere;
Reflux;
|
95%
|
|
With
N-chloro-succinimide;
In
chlorobenzene;
at 35 ℃;
for 3h;
Product distribution / selectivity;
Inert atmosphere;
|
77%
|
|
With
N-chloro-succinimide;
In
tetrachloromethane;
for 1h;
Heating;
Irradiation;
|
74%
|
|
With
tetrachloromethane; chlorine;
at -25 ℃;
|
|
|
With
sulfuryl dichloride; pentane;
|
|
|
With
sulfuryl dichloride;
In
dichloromethane;
for 1h;
Yield given;
Heating;
|
|
|
With
sulfuryl dichloride;
In
dichloromethane;
at 35 ℃;
for 0.5h;
|
|
|
With
sulfuryl dichloride;
Ambient temperature;
|
|
|
With
N-chloro-succinimide;
In
tetrachloromethane;
Ambient temperature;
|
|
|
With
N-chloro-succinimide;
In
tetrachloromethane;
|
|
|
With
sulfuryl dichloride;
In
dichloromethane;
|
|
|
With
N-chloro-succinimide;
In
tetrachloromethane;
at 0 ℃;
|
|
|
With
sulfuryl dichloride;
In
dichloromethane;
for 1h;
Yield given;
Heating;
|
|
|
With
N-chloro-succinimide;
In
tetrachloromethane;
at 20 ℃;
|
|
|
With
N-chloro-succinimide;
In
tetrachloromethane;
at 20 ℃;
|
|
|
With
sulfuryl dichloride;
In
dichloromethane;
at 50 ℃;
for 3h;
Inert atmosphere;
Reflux;
|
2.What is the CAS number for CHLOROMETHYL PHENYL SULFIDE ?
The CAS number of CHLOROMETHYL PHENYL SULFIDE is 7205-91-6.
More information of CHLOROMETHYL PHENYL SULFIDE 7205-91-6 are:
|
CAS?Number |
7205-91-6 |
|
Density |
1.2 g/cm3 |
|
Boiling Point |
275.6 °C at 760 mmHg |
|
Flash Point |
101.1 °C |
|
Vapor Pressure |
0.00847mmHg at 25°C |
|
Refractive Index |
n20/D 1.594(lit.) |
|
HS CODE |
29309099 |
|
PSA |
25.30000 |
|
LogP |
2.97500 |
3.What are another words for CHLOROMETHYL PHENYL SULFIDE ?
Synonyms?for?CHLOROMETHYL PHENYL SULFIDE 7205-91-6:Sulfide,chloromethyl phenyl (6CI,7CI,8CI);(Chloromethylthio)benzene;(Phenylthio)methyl chloride;Chloro(phenylthio)methane;Chloromethyl phenylsulfide;Chloromethyl phenyl thioether;NSC 203003;Phenyl chloromethylsulfide;a-Chlorothioanisole;
4.What is the molecular formula of CHLOROMETHYL PHENYL SULFIDE?
The chemical formula of ?CHLOROMETHYL PHENYL SULFIDE is?C7H7ClS which containing 7 Carbon atoms,7 Hydrogen atoms,1 Chlorine atoms and 1 Sulfur atoms,and the molecular weight of??CHLOROMETHYL PHENYL SULFIDE?is 158.652.
5.What is CHLOROMETHYL PHENYL SULFIDE (7205-91-6) used for?
CHLOROMETHYL PHENYL SULFIDE is an organic compound that serves as a reagent in the synthesis of various organic molecules, particularly α-methylene lactones and esters. It is known for its high-yield thiomethylation of O-silylated lactone and ester enolates, making it a valuable component in chemical reactions and pharmaceutical synthesis.
InChI:InChI=1/C7H7ClS/c8-6-9-7-4-2-1-3-5-7/h1-5H,6H2
Relevant articles related to CHLOROMETHYL PHENYL SULFIDE:
|
Article |
Source |
|
Consecutive C1-Homologation / Displacement Strategy for Converting Thiosulfonates into O,S-Oxothioacetals |
Ielo, Laura,Pillari, Veronica,Miele, Margherita,Holzer, Wolfgang,Pace, Vittorio , p. 5444 - 5449 (2020/10/12) |
|
An electrophilic reagent for the synthesis of OCHFMe-containing molecules |
Carbonnel, Elodie,Pannecoucke, Xavier,Besset, Tatiana,Jubault, Philippe,Poisson, Thomas supporting information, p. 2491 - 2493 (2018/03/21) |
6.Buy CHLOROMETHYL PHENYL SULFIDE with the best price .
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